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您所在的位置:> 儀器網 > 技術中心 > 使用手冊 > 微量水分測定儀的使用方法

微量水分測定儀的使用方法

2022年01月17日 14:28人氣:2367

  微量水分測定儀是研制的具有先進水平的現代化智能分析儀器,其主要是根據庫侖滴定原理,并以雙鉑電極檢測滴定過程,利用微型計算機進行自動控制電解和數據處理,具有操作便捷、分析速度快、電解速度快、靈敏度高、平衡時間短、結果準確等優點,廣泛應用于電力、化工、石油、醫藥、環保及科研等行業。
 
  微量水分測定儀的使用方法
 
  1.在測定開始前,需將滴定池內所有的玻璃扣打開,用水對滴定池、干燥管、密封塞進行清洗,洗凈后放入烘箱內烘干,隨后自然冷卻;
 
  2.將硅膠顆粒裝入干燥管中,旋塞轉好試樣注入口,隨后把攪拌子通過試樣注入口小心放入;
 
  3.在玻璃配件的毛玻璃部分均勻的涂一層真空潤滑脂,使其具有較好的密封效果;
 
  4.在電解池瓶內加入電解液至下端刻度線,再將大磨塞、測量電極、干燥管、進樣塞依次安裝完畢后,所有與電解池瓶有所接觸的部分都要涂抹真空潤滑脂,保證電解池的氣密性;
 
  5.在電解電極內添加電解液到與外部液面基本持平;
 
  6.將電解池放在微量水分測定儀的主機上,并接通電解電極插頭,組裝完畢后才能通電開機;
 
  7.進入測定界面后,將裝滿蒸餾水的50微升進樣器插到電解液液面以下,隨后慢慢注入蒸餾水,知道電解液完全變為淡黃色時便停止注水;
 
  8.電解質變為黃色后,測定儀會自動電解電解池中的水分直到平衡;
 
  9.根據測定儀的顯示屏提示,來判斷測定儀是否平衡;
 
  10.標定水分完成后,即可開始樣品的測定,使用一毫升的進樣器抽取一定量的待測樣品,點擊測定器的“開始”按鈕,測定器便會自動開始進行測定,直至完成。
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賽默飛 德國IKA
第7屆廣州國際生物技術大會暨展覽會
第7屆廣州國際生物技術大會暨展覽會

時間:2022.09.15~2022.09.17 地點:廣州·廣交會展館C區


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